Understanding Hardness Testing and its Applications

12, Aug. 2024

 

Understanding Hardness Testing and its Applications

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Clemex

In this interview, AZoM speaks with Clemex about hardness testing, the different types, and its various applications.

What is hardness testing?

Fundamentally, hardness testing determines the resistance a material exhibits in response to the permanent deformation of another material's penetration. If I take a piece of metal and rub something else against it, I would analyze how well the initial metal resists any deformation.

What are the typical or the most common applications for hardness testing?

Primarily the focus is on metals fabrication, pre and post-fabrication, as well as ceramics and composite materials. Hardness testing is always measured on anything subjected to heating, heat treatment, or materials bent or shaped into a product. It is an essential part of the manufacturing process.

What is a load cell and how do they work?

A load cell is a device that converts kinetic energy force into a measurable electrical signal. The advantage is that electrical signals are measurable and more accurate. We take a material, apply a force onto it, and it generates a small electrical signal which we then calibrate to the amplitude of the electrical signal to give us an idea of what sort of force we are applying. We sample this about a thousand times per second.

What kind of assemblies and applications would require a load cell in the testing setup?

A load cell is required in metal industry products, and where more accuracy is needed as opposed to a dead load system.

A dead load system is a series of plates with a specific weight placed on top of each other. These plates are introduced into the system to provide a certain force, but when that force is applied, it over-applies; for every action, there is an equal opposite reaction. The user applies what we call a little overshoot, and then it settles.

Load cells eliminate overshooting, providing a gentle approach, where the penetrator is placed onto the sample, held until it stabilizes, and then the force is increased so there is no overshooting of additional forces.

Image credit: Clemex

What customers, industries, and specific applications can make best use of load cells?

The heat treating industry is one of the largest industries using load cells. This industry alters the structure of metal, including ferrous and non-ferrous metals, as well as anything being heated, quenched, etc. This alters the microstructure of the materials, which simultaneously changes the hardness, tension, and other key properties.

Load cells are also used in the steel industry, where targeted specifications are known. It is also worth mentioning fabricators and industries where metal is bent or shaped and metal hardness is tested.

Can you talk us through the development process and the decisions that have led Clemex to produce this new offering?

The company was established around 32 years ago, and its product portfolio has always had a microhardness testing system. However, a dead load system was used for a long time, as this was the only type of testing approved by the American Standard Testing Methods (ASTM).

Around 10 years ago, ASTM began looking at some of these newer solutions, primarily load cell technologies. The main advantage is that you can program various experimental loads that can be used, and accuracy was the main driving force behind it. Now that it is an approved methodology within the ASTM or universal testing committees, Clemex is now selling load cell equipment.

What do you think your load cell solution brings to the market over what people might have tried already?

Load cell solutions bring ease of use and accuracy to the market. Clemex is sourcing the technology from a European manufacturer that has been in this business for over 65 years, and they have perfected this particular type of load cell.

The monitoring and sampling of the forces occur at times per second to deliver constant load values. This is the most significant and unparalleled advantage of this particular load cell technology.

This offers users a range of flexibility, from single to multiple samples, speed, accuracy, and the consultation that comes with the product from our growing expertise.

Can you explain what microhardness testing is as opposed to bulk harness testing?

There are four types of hardness testing in the market, Rockwell, Knoop, Vickers, and Brinell; these are the four scales we are working with.

Usually, Rockwell and Brinell are usually large, massive loads based on the penetration depth; a load is placed at zero point, and then the depth that this particular indenture will penetrate into the material is measured.

Microhardness testing is a little different. First, micro refers to looking at very small grains within the materials. We are not just testing the bulk metal, but we could be testing a crystal within that grain structure.

For example, if we measure a divot in both X and Y directions, and take an average, the formula is that the material and the indentation are inversely proportional to the displacement of the material.

If I have a larger impression, I have a soft material. If I have a smaller impression, I have a harder material. There are two main scales, Vickers and Knoop. Vickers is a symmetrical diamond shape, whereas Knoop is an elongated diamond.

Can you see a paradigm shift in how much testing people can get done because of the product's ease of use?

Absolutely. One of the biggest advantages is that you do not require a highly qualified user to run the software. It is extremely simple and user-friendly software. At the same time, we also have a greater throughput.

With some of the potential configurations of the microhardness testers, we can place up to 10 samples in them and set up what we call a traverse, a direction of how many indentations and how far apart we want them.

We can run that 10 times, place it on the auto-indexing table, and walk away. That means the operator can leave the hardness test unattended for three to four hours, and once the operator returns, they review the results.

Image credit: Clemex

Do you think there is any new application potential, or are there potential areas where people might start applying more rigorous testing that they were not able to get through before because of the difficulty or lack of throughput?

This depends on the end-user specifications, as we are finding more quality control in various industries, particularly automotive ones. Auto manufacturers now request more quality from their original parts suppliers, meaning they have to do more testing. Naturally, this means that the volumes will be increasing.

What is your vision for the future of the product? Are there any other developments that you would be looking at as things continue to change?

While these load cells are extremely accurate right now for what we require at the micro level, as we move forward, more high-tech materials are emerging and hitting the market.

In the future, we will need to go even lower and be more precise with the loads than we currently can. We are talking about nanotechnologies and nano loads. Having an exceptionally accurate load cell will lead us into that next area.

What kind of high-value applications and areas will you see requiring such improvements?

The automotive, electronic semiconductor, and pharmaceutical industries, where they are measuring tablet hardness. The applications will eventually go way beyond the metals industry.

What other challenges could come from adapting what is essentially developed as metals testing technology for softer materials?

Essentially, it is getting the industry to adapt and adopt. We have to prove to the industry that the results are just as good, if not better, than what they were used to, and get them to buy in and accept this technology.

We get to experience how a large number of manufacturers think and work. We visit different kinds of manufacturing plants, from steel to automotive, to baby formula, across various industries.

What kind of feedback have you received from customers so far?

Customers are very excited that we are advancing in this area and are looking forward to trying some of our instruments. We are looking forward to demonstrating them in the short term.

Clemex recently received excellent feedback at a metals show in Pittsburgh.

About Clemex

Clemex provides manufacturers and researchers with image analysis software and hardware to make quantification of microstructures less demanding and more effective. They specialize in automating measurement of objects in digital images from microscopes and other precision optical devices.

Clemex's strength lies in their ability to achieve a thorough understanding of their clients' specific applications, leading to a high satisfaction rate among Clemex customers. Major quality control and research labs all over the world use our image analysis solutions to extract meaningful size, shape and volume measurements in applications as varied as particle shape analysis, heat-affected zone (HAZ) measurements in welds, fiber length and morphology, automated microhardness testing, and automated inclusion rating in steel.

 

This information has been sourced, reviewed and adapted from materials provided by Clemex Technologies.

For more information on this source, please visit Clemex Technologies.

Disclaimer: The views expressed here are those of the interviewee and do not necessarily represent the views of AZoM.com Limited (T/A) AZoNetwork, the owner and operator of this website. This disclaimer forms part of the Terms and Conditions of use of this website.

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Hardness testing

Ted Stroud
QA / QC United Kingdom, Joined Jul ,
2
Ted Stroud
QA / QC
United Kingdom,
Joined Jul
2

QA / QCUnited Kingdom,Joined Jul

09:37 Jul-20-
Hardness testing 09:37 Jul-20-

I am currently introducing in-house raw material hardness testing. I am using a Foundrax Model 134 Portable Brinell Hardness Tester to undertake the work. I have about a 600mm x 120mm throat size. My average raw bar Ø are around 8”-10” and approximately 12”- 20” long.
My procedure calls for 4 test points on each end of the material.

As i am pretty new to this field, my question is has anyone got any good solutions to the best way of setting up to undertake the physical testing. Currently i set the hardness tester on its side using V blocks and role the material into the throat, working at floor level.

Really I am looking for some inspiration to make the process as safe and efficient as possible. Any suggestions gratefully received.

Nigel Armstrong
Engineering, - Specialist services United Kingdom, Joined Oct ,

Nigel Armstrong
Engineering, - Specialist services
United Kingdom,
Joined Oct

Engineering, - Specialist servicesUnited Kingdom,Joined Oct

20:52 Jul-21-
Re: Hardness testing 20:52 Jul-21-
In Reply to Ted Stroud at 09:37 Jul-20- (Opening).

Ted

I have never handled the Foundrax 134 but having checked their website I can see why you are struggling.

You say you are new to the field so are you aware of machines such as the MicroDur, MIC 10 or Equotip? These machines are ideal for your application of solid bars. They work on rebound dynamics and the probe is connected to the electronics by a cable so its eaasily manipulated and can convert electronically to many different hardness tables . Have a look at GE Instruments for their catalogue or Google Equotip.

Sorry I cant help with manipulation of the Foundrax.

Vicky
NDT Inspector, Blue Star Limited IE , India, Joined May ,
29
Vicky
NDT Inspector, Blue Star Limited
IE ,
India,
Joined May
29

NDT Inspector, Blue Star LimitedIE ,India,Joined May

11:02 Jul-25-
Re: Hardness testing 11:02 Jul-25-
In Reply to Nigel Armstrong at 20:52 Jul-21- .

Hi Ted,
I fully aggree with the post of Mr Nigel as far as your job & your procedure discription is concerned making use of Equitip or any rebound type hardness tester are very effective, since you are also intrested in taking only point measurements its the best suit for you.


regards

Vignesh M

Michael Lewis
NDT Inspector, Quality Manager Tejas Testing & Inspection, USA, Joined Mar ,
10
Michael Lewis
NDT Inspector, Quality Manager
Tejas Testing & Inspection,
USA,
Joined Mar
10

NDT Inspector, Quality ManagerTejas Testing & Inspection,USA,Joined Mar

18:46 Jul-26-
Re: Hardness testing 18:46 Jul-26-
In Reply to Ted Stroud at 09:37 Jul-20- (Opening).

Be aware that most end users do not accept Equotip or similar rebound testers as a valid hardness test. They allow you to use it for sorting purposes, but not for final inspection. So before you go blowing a few thousand dollars on some equotip machine, keep in mind that half the procedures out there specifically ban it and your customers may be asking for it to get retested in many cases.

Also, I have never heard of setting the hardness tester "on it's side." I would check with manufacturer to make sure it is an allowable practice. The standards I work with do not address this configuration and it would be worth checking to see if your load can be applied properly when horizontal.

Another idea that I have played around with but haven't put into practice (I don't do HBW often enough) uses pipe racks and a chair. In a warehouse setting (smooth, level flooring), you could put the material on pipe racks. Get an office chair (or similar apparatus to your imagination) and put the hardness tester on the seat of it. Maybe get rid of the seat entirely and use a flat piece of plywood. Anyhow, the idea is to use the feature of many office chairs that allows it to raise up and down. Then you can secure the tester to the chair and adjust the height to match the bars. Final step would be to wheel the tester around to the bar (instead of rolling the bar) and you would save your back and some sweat.

Someone let me know if that idea is ridiculous so I know to whether to try it myself or not.

Nigel Armstrong
Engineering, - Specialist services United Kingdom, Joined Oct ,

Nigel Armstrong
Engineering, - Specialist services
United Kingdom,
Joined Oct

Engineering, - Specialist servicesUnited Kingdom,Joined Oct

01:45 Jul-27-
Re: Hardness testing 01:45 Jul-27-
In Reply to Michael Lewis at 18:46 Jul-26- .

Ted

You are in the UK so this may not apply - it depends on the contractual soecification, if any. ASTM specification A-956 Equotip Hardness Testing of Metallic Materials has been around for 10 years. You say you are introducing hardness testing so it seems you arre calling the shots. As such im certain if you demonstrate compliance with A-956 it would be a very bloody-minded end user who would not sanction its use

Your application of heavy steel bars is ideally suited for its use. By rolling the bar so you are always testing at 12 o'clock you will optimise test accuracy. I would prefer you to use Equotip in the proper way than the Foundrax in a manner it was not designed for.

Hope this helps

Ted Stroud
QA / QC United Kingdom, Joined Jul ,
2
Ted Stroud
QA / QC
United Kingdom,
Joined Jul
2

QA / QCUnited Kingdom,Joined Jul

08:53 Jul-27-
Re: Hardness testing 08:53 Jul-27-
In Reply to Ted Stroud at 09:37 Jul-20- (Opening).

I would like to thank you guys for giving me food for thought. I have already got an EQUOTIP in my inspection department. As stated some specs prohibit the use of the equipment, but I am interested in doing comparisons in the results achieved.

Nigel Armstrong
Engineering, - Specialist services United Kingdom, Joined Oct ,

Nigel Armstrong
Engineering, - Specialist services
United Kingdom,
Joined Oct

Engineering, - Specialist servicesUnited Kingdom,Joined Oct

09:51 Jul-27-
Re: Hardness testing 09:51 Jul-27-
In Reply to Ted Stroud at 08:53 Jul-27- .

Good morning Ted

The 06 editon of A-956 has been renamed (maybe to move away from the proprietary Equotip name in its title) to Standard test Method for Leeb Hardnes testing. I dont have the newer version, but I believe it still relates to the Equotip Method.

For the MIC 10/20 and other UCI instruments, ASTM A- Standard Practice for Portable Hardness Testing by the Ultasonic Contact Impedance Method

I should have perhaps been a bit more circumspect in my OP as Michael pointed out as oth methods do only measure surface hardness and not bulk hardness that will be measured by an indentor. So it usage would depend on the material condition. However the referenced ASTMs standardise the methods to give them much more credibility when used properly.

If you are tied by specifications to use of an indentor method then the above are of no use unless their use ic conceded. But as Michael points out use of an indentor lying on its side is hardly kosher! I hope you fiind a convenient solution to your predicament.

S.V.Swamy
Engineering, - Material Testing Inspection & Quality Control Retired from Nuclear Fuel Complex , India, Joined Feb ,
787 3
S.V.Swamy
Engineering, - Material Testing Inspection & Quality Control
Retired from Nuclear Fuel Complex ,
India,
Joined Feb
787 3

Engineering, - Material Testing Inspection & Quality ControlRetired from Nuclear Fuel Complex ,India,Joined Feb

16:04 Jul-27-
Re: Hardness testing 16:04 Jul-27-
In Reply to Nigel Armstrong at 09:51 Jul-27- .

Dear Friends,

I was following the discussion with a lot of interest. In my own long career, I had the good opportunity to perform hardness testing of zircaloy and steel bars / billets etc. on the shop floor (yes, I did the initial testing with my own hands and then trained the technicians to use it). We had all the different methods that are being discussed. Indentation, rebound, spring / hydraulic driven / ultrasonic...

C type indentation hardness testers that depend on screw / hydraulic pressure can be used in horizontal position. I checked the Foundrax website and they clearly mention that the model 134 can be used in any position, implying that it is not gravity driven!

Since they use the standard indenters and apply the full load, they meet the hardness testing specifications / standards fully.

Superficial / surface indentation testers and rebound testers, ultrasonic testers etc. give the surface hardness, which may or may not represent the internal hardness of the material. Only machined bars and billets probably satisfy the condition where the surface hardness is close to the internal hardness. If the bars are having scale, we may need to grind a few spots and check those spots.

Regards.

S.V.Swamy
Quality Consultant

Simon Amallraja
Simon Amallraja
17:55 Jul-27-
Re: Hardness testing 17:55 Jul-27-
In Reply to Ted Stroud at 09:37 Jul-20- (Opening).

You can also try Ultrasonic mode of Case Hardening, using UT Equipment with related Software meant for Hardness Measurement.

There are many manufacturers and you can check for Autoscan or . You need to check the details and decide as per your reqt

Simon

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